Commission regulation (EC) No 1623/2000 of 25 July 2000 laying down detailed rules for implementing Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms
Modified by
- Commission Regulation (EC) No 2409/2000of 30 October 2000amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 300R2409, October 31, 2000
- Commission Regulation (EC) No 2786/2000of 19 December 2000amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 300R2786, December 20, 2000
- Commission Regulation (EC) No 545/2001of 20 March 2001amending Regulation (EC) No 1623/2000 laying down certain detailed rules for implementing Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 301R0545, March 21, 2001
- Commission Regulation (EC) No 1282/2001of 28 June 2001laying down detailed rules for the application of Council Regulation (EC) No 1493/1999 as regards the gathering of information to identify wine products and to monitor the wine market and amending Regulation (EC) No 1623/2000, 301R1282, June 29, 2001
- Commission Regulation (EC) No 1660/2001of 16 August 2001amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 301R1660, August 17, 2001
- Commission Regulation (EC) No 2022/2001of 15 October 2001amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 301R2022, October 16, 2001
- Commission Regulation (EC) No 2047/2001of 18 October 2001amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 301R2047, October 19, 2001
- Commission Regulation (EC) No 2429/2001of 12 December 2001amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms and amending Regulation (EC) No 442/2001 opening crisis distillation as provided for in Article 30 of Council Regulation (EC) No 1493/1999 for table wines in Portugal, 301R2429, December 13, 2001
- Commission Regulation (EC) No 2464/2001of 14 December 2001amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 301R2464, December 15, 2001
- Commission Regulation (EC) No 1315/2002of 19 July 2002amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 302R1315, July 20, 2002
- Commission Regulation (EC) No 1795/2002of 9 October 2002amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 302R1795, October 10, 2002
- Commission Regulation (EC) No 625/2003of 2 April 2003amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 303R0625, April 8, 2003
- Commission Regulation (EC) No 1183/2003of 2 July 2003amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 303R1183, July 3, 2003
- Commission Regulation (EC) No 1411/2003of 7 August 2003amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 303R1411, August 8, 2003
- Commission Regulation (EC) No 1710/2003of 26 September 2003amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 303R1710, September 27, 2003
- Commission Regulation (EC) No 908/2004of 29 April 2004adapting several regulations concerning the common organisation of the market in wine by reason of the accession of the Czech Republic, Estonia, Cyprus, Latvia, Lithuania, Hungary, Malta, Poland, Slovenia and Slovakia to the European Union, 304R0908, April 30, 2004
- Commission Regulation (EC) No 1774/2004of 14 October 2004amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 304R1774, October 15, 2004
- Commission Regulation (EC) No 535/2005of 6 April 2005correcting the Italian version of Regulation (EC) No 1623/2000 laying down detailed rules for implementing Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 305R0535, April 7, 2005
- Commission Regulation (EC) No 616/2005of 21 April 2005amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 305R0616, April 22, 2005
- Commission Regulation (EC) No 1219/2005of 28 July 2005amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 305R1219, July 29, 2005
- Commission Regulation (EC) No 1820/2005of 8 November 2005amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 305R1820, November 9, 2005
- Commission Regulation (EC) No 1221/2006of 11 August 2006amending Regulation (EC) No 1623/2000 laying down detailed rules for implementing Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 306R1221, August 12, 2006
- Commission Regulation (EC) No 1713/2006of 20 November 2006abolishing the prefinancing of export refunds in respect of agricultural products, 306R1713, November 21, 2006
- Commission Regulation (EC) No 2016/2006of 19 December 2006adapting several regulations concerning the common organisation of the market in wine by reason of the accession of Bulgaria and Romania to the European Union, 306R2016, December 29, 2006
- Commission Regulation (EC) No 897/2007of 27 July 2007amending Regulation (EC) No 1623/2000 laying down detailed rules for the application of Council Regulation (EC) No 1493/1999 on the common organisation of the market in wine with regard to market mechanisms, 307R0897, July 28, 2007
- Commission Regulation (EC) No 923/2007of 1 August 2007amending Regulation (EC) No 1623/2000 as regards certain deadlines for the distillation of the by-products of winemaking, 307R0923, August 2, 2007
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(a) being themselves producers or groups of producers, process or have processed on their behalf grapes from their own harvest and grape must and concentrated grape must obtained entirely from their own grape crop into grape juice; or (b) buy directly or indirectly from producers or groups of producers grapes produced in the Community and grape must and concentrated grape must for the purpose of processing them into grape juice.
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(a) the type of the raw materials intended for processing (grapes, grape must or concentrated grape must); (b) the place where the grape must and concentrated grape must intended for processing are stored; (c) the place where processing is to be carried out.
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(a) the information required under the second subparagraph of paragraph 1; (b) the quantity of grapes, grape must or concentrated grape must intended for processing; (c) the density of the grape must and concentrated grape must; (d) the starting date and probable duration of processing operations.
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(a) 1,3 tonnes for grapes; (b) 10 hectolitres for grape must; (c) 3 hectolitres for concentrated grape must.
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(a) the quantities and the density of the raw materials entering their premises each day and, where applicable, the name and address of the seller; (b) the quantities and density of raw materials used each day; (c) the quantities of grape juice produced each day; (d) the quantities of grape juice leaving their premises each day and the name and address of the consignee, or the quantities of grape juice used each day by the processor.
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(a) processors shall indicate on the accompanying document referred to in Article 70(1) of Regulation (EC) No 1493/1999 whether the manufacture of the grape juice has been or will be subject to an aid application from them and the actual or planned date of submission of the application; (b) users shall send the accompanying document to the competent authority of the place of unloading no later than 15 days after receipt of the product; (c) where users dispatch the juice they have received to another operator within the Community they shall ensure that that operator signs their written undertaking and shall submit it to the competent authority within the time limit set in the second subparagraph of paragraph 2; (d) the competent authority, after having received the written undertaking, shall stamp the accompanying document and send a copy of the stamped accompanying document to the processor of the grape juice in question no later than 30 days after receipt of the undertaking.
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(a) a copy of the processing schedule referred to; (b) a copy of the stock records referred to in Article 6(6) or a summary thereof; the Member States may require such copies and summaries to be certified by an authority responsible for inspections.
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(a) a copy of the processing statement referred to; (b) a copy of the stock records referred to in Article 6(6) or a summary thereof; the Member States may require such copies and summaries to be certified by an authority responsible for inspections.
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(a) a copy of the accompanying document stamped by the competent authority as laid down in Article 7(3)(d); (b) a copy of the accompanying document bearing the customs stamp certifying export.
EUR 4,952 per 100 kg; | |
EUR 6,193 per hl; | |
EUR 21,655 per hl. |
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(a) 1,3 for grapes, in 100 kg per hl; (b) 1,05 for must, in hl per hl; (c) 0,30 for concentrated must, in hl per hl.
(a) Concentrated grape must from grapes harvested: -
in wine-growing zones C III (a) and C III EUR 1.699/% vol./hl elsewhere EUR 1.466/% vol./hl
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(b) Rectified concentrated grape must from grapes harvested: -
in wine-growing zones C III (a) and C III EUR 2.206/% vol./hl elsewhere EUR 1.955/% vol./hl
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(a) to manufacturers who use concentrated grape must obtained entirely from grapes produced within wine-growing zones C III (a) and C III (b) for the manufacture in the United Kingdom and Ireland of products falling within CN code 220600 for which the use of a composite name including the word "wine" may be allowed by these Member States under Annex VII(C)(3) to Regulation (EC) No 1493/1999, hereinafter called "manufacturers". The amount of the aid shall be EUR 0.2379 per kilogram; (b) to operators who use concentrated grape must obtained entirely from grapes produced in the Community as the main component in a set of products which they market in the United Kingdom and Ireland, with clear instructions enabling the consumer to obtain therefrom a beverage in imitation of wine, hereinafter called "operators". The amount of the aid shall be EUR 0.3103 per kilogram.
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(a) the name or business name and the address of the manufacturer or operator; (b) the wine-growing zone from which the concentrated grape must originates, as defined in Annex III to Regulation (EC) No 1493/1999; (c) the following technical information: -
(i) the place of storage, (ii) the quantity (in kilograms or, if the concentrated grape must referred to in Article 35(1)(c) of Regulation (EC) No 1493/1999 is put up in containers with contents not exceeding 5 kilograms, the number of containers), (iii) the density, (iv) the prices paid, (v) the place where the operations referred to in Article 35(1)(b) and (c) of Regulation (EC) No 1493/1999 are carried out.
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(a) the consignments of concentrated grape must purchased and brought each day into their premises, together with the information indicated in Article 19(2)(b) and (c) of this Regulation and the name and address of the seller(s), (b) the quantities of concentrated grape must used each day for the purposes referred to in Article 35(1)(b) and (c) of Regulation (EC) No 1493/1999, (c) the consignments of finished products mentioned in Article 35(1)(b) and (c) of Regulation (EC) No 1493/1999 produced and dispatched each day from their premises, together with the name and address of the consignee(s).
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(a) EUR 0.01837 for grape must; (b) EUR 0.06152 for concentrated grape must; (c) EUR 0.06152 for rectified concentrated grape must; (d) EUR 0.01544 for table wines.
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(a) the processing of fresh grapes into grape must, (b) the processing of grape must into concentrated grape must or rectified concentrated grape must, (c) the processing of fresh grapes, grape must or grape must in fermentation into table wine.
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produced by them, or produced on their responsibility and which they own, or in the case of producer organisations as referred to in the third subparagraph of paragraph 1, produced on the responsibility of their members.
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(a) the grape musts concerned must have been obtained exclusively from varieties classified as wine grapes in accordance with Article 19 of Regulation (EC) No 1493/1999 and may not have a natural alcoholic strength by volume lower than the minimum natural alcoholic strength laid down for the wine-growing zone in which they originate, (b) table wines: -
(i) must comply with the minimum quality requirements fixed in Annex II to this Regulation for the category for which the contract is concluded; (ii) must have a reducing sugar content not greater than two grams per litre, except in the case of table wines from Portugal, which must have a reducing sugar content not greater than four grams per litre; (iii) must display a satisfactory 24-hour exposure to air, (iv) must be free of bad tastes.
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(c) The radioactivity levels of the products referred to in Article 24 of this Regulation may not exceed the maximum levels permitted under Community rules. However, the level of radioactive contamination of products shall be monitored only if the situation so requires and only during the period necessary.
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(a) details enabling the product to be identified, (b) the following analysis data: (i) the colour, (ii) the sulphur dioxide content, (iii) the absence of hybrids, in the case of red products, as demonstrated by analysis for malvidol diglucoside.
(c) the reading obtained at a temperature of 20 o C with a refractometer used in accordance with the method referred to in the Annex to Regulation (EEC) No 558/93. A tolerance shall be permitted of 0,5 for grape must and 1 for concentrated grape must and rectified concentrated grape must.
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(d) the total alcoholic strength by volume, (e) the actual alcoholic strength by volume, (f) the total acidity, expressed in grams of tartaric acid per litre or in milliequivalents per litre; however, Member States may waive this requirement for white wines, (g) the volatile acid content, expressed in grams of acetic acid per litre or in milliequivalents per litre; however, Member States may waive this requirement for white wines, (h) the reducing sugar content, (i) behaviour in air over 24 hours, (j) the absence of bad tastes.
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(a) the name and address of the producers concerned, (b) the name and address of the intervention agency, (c) the type of product, classified as indicated in Article 25 of this Regulation, (d) the quantity, (e) the place of storage, (f) the first day of the storage period, (g) the amount of aid in euros.
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(h) a statement that the first racking has taken place, (i) a clause to the effect that the volume may be reduced by a percentage to be determined by the Commission in accordance with the procedure laid down in Article 75 of Regulation (EC) No 1493/1999 should the total volume covered by contracts significantly exceed the average volumes covered in the last three wine years; such reduction may not reduce the quantities in storage below the minimum levels referred to in Article 28(2). Where this clause is applied, the full amount of the aid due for the period prior to the reduction shall remain payable.
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(a) must comply with the relevant definitions in Annex I to Regulation (EC) No 1493/1999, (b) must retain at least the minimum alcoholic strength required for the category of table wine concerned at the time of conclusion of the contract, (c) may not be kept in containers of less than 50 litres capacity, (d) must remain in bulk, and (e) in the case of wine, must remain fit for offer or supply for direct human consumption at the end of the storage period.
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(a) in the place of storage, or (b) in the manner in which the product is put up. In such cases, they shall indicate the containers in which the product is to be definitively stored.
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(a) the amount referred to in Article 25(a) of this Regulation for the processing referred to in the first subparagraph of paragraph 6, (b) the amount referred to in Article 25(b) of this Regulation for the processing referred to in the second subparagraph of paragraph 6.
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(a) where producers fail to fulfil their obligations under Article 34(1) to (5) and (7) of this Regulation or refuse to submit to checks, no aid shall be payable; (b) where producers fail to fulfil one of their obligations under this Regulation or under the contract, other than those referred to in (a) above, the aid shall be reduced by an amount determined by the competent authority depending on the seriousness of the infringement.
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(a) "producer" means: -
(i) for the purposes of Chapter I of this Title: any natural or legal person or group of such persons having produced wine from fresh grapes, grape must or partially fermented grape must or from new wine still in fermentation, obtained personally or purchased, or any natural or legal person or group of such persons subject to the obligations referred to in Article 27 of Regulation (EC) No 1493/1999; (ii) for the purposes of Chapters II and III of this Title: any natural or legal person or group of such persons having produced wine from fresh grapes, grape must or partially fermented grape must, obtained personally or purchased;
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(b) "distiller" means any natural or legal person or group of such persons: -
(i) distilling wine, wine fortified for distillation or the by-products of wine-making or of any other form of processing grapes, and (ii) approved by the competent authorities in the Member State in whose territory the distillation premises are located;
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(c) "maker of wine fortified for distillation" means any natural or legal person or group of such persons, other than distillers: -
(i) processing wine into wine fortified for distillation, and (ii) approved by the competent authorities in the Member State in whose territory the premises are located;
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(d) "competent intervention agency" means: -
(i) for the purposes of receiving and approving contracts or declarations relating to the delivery of wine for distillation and receiving and approving contracts relating to the delivery of wine for fortification, the intervention agency designated by the Member State in whose territory the wine is located at the time when the contract or declaration is submitted, (ii) for the purposes of paying aid to makers of wine fortified for distillation under Article 69, the intervention agency designated by the Member State in whose territory the wine is fortified, (iii) in all other cases, the intervention agency designated by the Member State in whose territory distillation takes place.
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(a) are approved by the competent authorities in the Member State in which they are established; (b) buy from a producer as defined in paragraph 1(a) wine or the by-products of wine-making or of any other form of processing of grapes with a view to having them distilled on their own account by an approved distiller, and (c) pay the producer not less for the products purchased than the minimum buying-in price for the distilled product in question.
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(a) member cooperatives may not individually sign distillation contracts or make deliveries for the distillation concerned, (b) the quantities of wine delivered for distillation by the said association shall be booked to the member cooperatives on whose behalf the delivery is made.
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(a) neutral alcohol complying with the definition in Annex III to this Regulation, or (b) spirits distilled from wine or from grape marc, complying with the definitions in Article 1(4)(d) or (f) of Council Regulation (EEC) No 1576/89 of 29 May 1989 laying down general rules on the definition, description and presentation of spirit drinks , orOJ L 160, 27.6.1989, p. 1 . Last amended by Regulation (EC) No 3378/94 (OJ L 366, 31.12.1994, p. 1 ).(c) a distillate or raw alcohol with an alcoholic strength of at least 52 % by volume.
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(i) the production of an alcoholic beverage, (ii) processing into one of the products referred to in (a) or (b) above, with the exception of spirits distilled from grape marc, (iii) the production of alcohol for industrial purposes.
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(a) all of their marc and wine lees to an approved distiller, and (b) where applicable, any wine to an approved distiller or approved maker of wine fortified for distillation.
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(a) 8.5 % for zone B, (b) 9.0 % for zone C I, (c) 9.5 % for zone C II, (d) 10.0 % for zone C III,
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(a) grape marc: -
(i) in wine-growing zone B: two litres of pure alcohol/100 kilograms, (ii) in wine-growing zone C: two litres of pure alcohol, by actual or potential strength/100 kilograms where it is obtained from varieties listed in the classification of vine varieties for the administrative unit concerned as varieties other than wine-grape varieties; litres of pure alcohol, by actual or potential strength/100 kilograms where it is obtained from varieties listed in the classification for the administrative unit concerned solely as wine-grape varieties;
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(b) wine lees: -
(i) in wine-growing zone B: three litres of pure alcohol/100 kilograms, 45 % moisture content, (ii) in wine-growing zone C: four litres of pure alcohol/100 kilograms, 45 % moisture content,
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(a) pay the producer on account 80 % of the buying-in price, no more than three months after delivery of the products, or (b) make the payment on account referred in (a) following delivery of the products and no later that one month after presentation of the invoice to be drawn up for them before 31 August following the close of the wine year concerned.
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(a) for neutral alcohol: -
obtained from marc: EUR 0,8453, obtained from wine and wine lees: EUR 0,4106;
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(b) for spirits distilled from marc and distillates or raw alcohol obtained from marc having an alcoholic strength of at least 52 % vol.: EUR 0,3985; (c) for wine spirits and raw alcohol obtained from wine and wine lees: EUR 0,2777.
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(a) producers who withdraw by-products of wine-making under supervision under Article 50(1) of this Regulation, (b) producers of quality sparkling wines of the aromatic type and quality sparkling wines and semi-sparkling wines of the aromatic type produced in specified regions who have prepared such wines from grape must or partially fermented grape must which has been purchased and stabilised to eliminate the wine lees.
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(a) producers who produce no more than 80 hl by themselves on their own premises; (b) producers who grow their grapes using organic production methods.
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(a) those established in production areas where distillation is a disproportionate constraint. A list of the production areas concerned shall be drawn up by the competent authorities of the Member States, who shall inform the Commission thereof; (b) those who have not made wine or processed grapes in any other way on cooperative premises and who have disproportionate distillation costs on account of their low volume of production or the special characteristics of production and the location of the distilleries. The Member State shall lay down the detailed rules of application for this point and inform the Commission thereof.
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(a) grape marc: -
(i) 2.1 litres/100 kilograms in the case of quality white wines psr, (ii) 3 litres/100 kilograms in other cases.
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(b) wine lees: -
(i) 3.5 litres/100 kilograms in the case of quality white wines psr, (ii) 5 litres/100 kilograms in other cases.
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wine products intended for the production of table wine and wine suitable for yielding table wine, must intended for the production of concentrated must and rectified concentrated must for the purposes of enrichment, must intended for the production of liqueur wines with a designation of origin, wine products for the production of spirits distilled from wine with a designation of origin.
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1974/75 to 1979/80 in the Community of Ten, 1978/79 to 1983/84 in Spain and Portugal, 1988/89 to 1993/94 in Austria, 1997/98 to 2002/03 in the Czech Republic, Cyprus, Hungary, Malta, Slovenia and Slovakia, 1999/2000 to 2004/2005 in Romania.
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the Member State shall apportion the total quantity of wine to be distilled in the region concerned among the individual wine producers in that region in accordance with objective criteria and without discrimination and shall inform the Commission thereof, distillation shall be authorised only if the total quantity intended for wine-making in the region in the wine year concerned exceeds the total quantity normally produced in the region concerned, for each wine year a difference of 200000 hectolitres shall be allowed between the regional quantity to be distilled and the aggregate individual quantities.
(a) neutral alcohol: | EUR |
(b) spirits distilled from wine, raw alcohol and wine distillate: | EUR |
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(a) a customs office for completion of customs export formalities followed by departure from the customs territory of the Community, or (b) the premises of an approved maker of wine fortified for distillation with a view to fortification.
(a) the buying-in price for remaining quantities as indicated in the first subparagraph and the price for the alcohol produced from them and delivered to the intervention agency shall be reduced by EUR 0,6279/% vol of alcohol and per hectolitre in the case of distillation as indicated in Article 27 of Regulation (EC) No 1493/1999 and by EUR 0,7728/% vol of alcohol and per hectolitre in the case of distillation as indicated in Article 28 of that Regulation, (b) no aid shall be paid for products of distillation not delivered to intervention agencies, (c) the obligation shall be deemed to have been discharged by the date fixed in accordance with the first subparagraph, (d) the time limits for distillation, submission of proof of payment of the price referred to at (a) and delivery of the alcohol to the intervention agency shall be adjusted by the competent authority to take account of the extended time limit for delivery.
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a) -
(i) in the case of wine and wine lees, a summary of the deliveries made by each producer, stating at least: -
the type, quantity, colour and alcoholic strength by volume, the number of the document provided for in Article 70(1) of Regulation (EC) No 1493/1999, where such a document is required for transport of the products to the distiller's premises or, otherwise, the reference number of the transport document used under national rules;
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(ii) in the case of grape marc, a list of the names of the producers who have delivered marc and the quantity of alcohol contained in the marc delivered for distillation under Article 27 of Regulation (EC) No 1493/1999;
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(b) a declaration, stamped by the competent authority designated by the Member State, stating at least: -
(i) the quantity of products obtained by distillation, broken down by category as indicated in Article 43 of this Regulation, (ii) the date on which these products were obtained;
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(c) proof that they have paid the producer the minimum buying-in price laid down for the distillation operation concerned within the time allowed.
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(a) the type, quantity, colour and alcoholic strength by volume of the product to be distilled, (b) the quantity of products obtained from distillation, broken down by category as indicated in Article 43 of this Regulation, (c) the dates on which these products were obtained.
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(a) distillation under Article 27 of Regulation (EC) No 1493/1999: -
raw alcohol obtained from marc: EUR 1,872, raw alcohol obtained from wine and wine lees: EUR 1,437;
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(b) distillation under Article 28 of Regulation (EC) No 1493/1999: -
raw alcohol obtained from wine: EUR 1,799.
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(a) may be decided on by the Member States where application of the standard price makes it or could make it impossible to have one or more of the by-products of wine-making distilled in certain regions of the Community, (b) must be paid to distillers where one of these raw materials accounts for more than 60 % of the total quantities they have distilled during a given wine year.
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for the entire quantity if the Commission has not set the reduction percentage referred to in paragraph 5, for the quantity resulting from application of the reduction percentage if one has been set.
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EUR 1,751/% vol/hl for raw alcohol, wine distillate and spirits distilled from wine, EUR 1,884/% vol./hl for neutral alcohol.
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for at least 100 hectolitres of product obtained from distillation stored in containers of a capacity of at least 100 hectolitres, and for no less than six months and no more than 12 months. From the seventh month, distillers who have not claimed the advance referred to in Article 66 of this Regulation may terminate the contract in advance by specifying the final date in a statement addressed to the competent authority at least one month before the chosen date.
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(a) the quantity, which may not be less than 10 hectolitres, (b) the various characteristics, and in particular colour.
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(a) in the case referred to in the first subparagraph of paragraph 3, by the declaration, (b) in the case referred to in the second subparagraph of paragraph 3, by the declaration accompanied by a contract for delivery for distillation on the producer's behalf concluded between the producer and the distiller.
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(a) if the quantity of wine actually delivered for distillation is less than 95 % of that stated in the contract or declaration; (b) for any quantity of wine in excess of 105 % of that stated in the contract or declaration; (c) for any quantity of wine over and above the maximum quantity to be complied with for the distillation operation in question.
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(a) details of the quantity, colour and actual alcoholic strength by volume of the wine in each delivery from each producer from whom they have received deliveries of wine, together with the number of the document provided for in Article 70 of Regulation (EC) No 1493/1999 used for the transport of the wine to the distiller's premises; (b) proof that the total quantity of wine stipulated in the contract or declaration has been distilled within the time allowed; (c) proof that they have paid the producer the purchase price referred to in paragraph 6 within the time allowed.
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(a) that the producer has actually produced and holds the quantity of wine to be delivered, (b) that the wine entered in the contract belongs to the category for which distillation has been opened.
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(a) the document(s) and register(s) required under Article 70 of Regulation (EC) No 1493/1999 shall show the increase in actual alcoholic strength by volume, expressed in % vol., by indicating the strength before and after addition of the distillate to the wine, (b) a sample of the wine shall be taken under official supervision before it is fortified so that the actual alcoholic strength by volume may be determined by an official laboratory or a laboratory working under official supervision, (c) two copies of the report on the analysis referred to in (b) shall be sent to the manufacturer of the fortified wine, who shall transmit one copy to the intervention agency of the Member State in which the wine is fortified.
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(a) free at maker's premises in the case of distillation under Article 27(9) of Regulation (EC) No 1493/1999, (b) ex producer's premises in other cases.
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EUR 0.2657 for distillation as provided for in Article 27 of Regulation (EC) No 1493/1999; EUR 0.6158 for distillation as provided for in Article 28 of Regulation (EC) No 1493/1999; EUR 0.1715 for distillation as provided for in Article 29 of Regulation (EC) No 1493/1999.
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(a) of proof that the total quantity of wine fortified for distillation indicated in the contract or declaration has been distilled within the time allowed, and (b) of proof that the minimum purchase price referred to in Articles 27, 28, 29 and 30 of Regulation (EC) No 1493/1999 has been paid within the time allowed.
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(a) a document, endorsed by the competent authorities of the Member State in whose territory the wine was fortified, transferring entitlement to the aid from the maker of the fortified wine to the distiller and showing the quantities of fortified wine concerned and the amount of the corresponding aid, (b) a copy of the contract or declaration referred to in Article 69(1), approved by the competent intervention agency, (c) a copy of the analysis report referred to in Article 68, (d) proof that the minimum purchase price of the wine has been paid to the producer, (e) the document required under Article 70 of Regulation (EC) No 1493/1999 for the transport of fortified wine to the distillery, showing the increase in actual alcoholic strength by volume, expressed in % vol., by indicating the strength before and after addition of the distillate to the wine, (f) proof that the fortified wine concerned has been distilled.
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(a) if the force majeure affected the product to be distilled while it was legally at the disposal of the producer, the latter shall inform the intervention agency of the Member State in which the winery is located without delay, (b) in all other cases, the distiller shall inform the intervention agency of the Member State in which the distillery is located without delay.
-
(a) the document provided for in Article 70 of Regulation (EC) No 1493/1999 under cover of which the products are transported, (b) an analysis of samples collected under the supervision of an official body of the Member State in which the distillery is located when the product enters the distillery. Sampling may take the form of representative spot checks, (c) where appropriate, the contracts concluded under this Title.
-
(a) no aid shall be due for the quantities concerned, (b) the distiller may not deliver the products obtained by distilling the quantities concerned to the intervention agency.
-
(a) failure to present the harvest, production or stock declaration within the time allowed; (b) presentation of a harvest, production or stock declaration found by the competent authority of the Member State to be incomplete or inaccurate, where the missing or incorrect data are essential for application of the measure concerned; (c) failure to meet the obligations laid down in Article 37 of Regulation (EC) No 1493/1999 where the infringement is detected or notified to the distiller after payment of the minimum price on the basis of previous declarations.
-
(a) where producers fail to fulfil their obligations under this Title or refuse to submit to checks, no aid shall be payable; (b) where distillers fail to fulfil one of their obligations other than those referred to in (a) above, the aid shall be reduced by an amount determined by the competent authority depending on the seriousness of the infringement.
-
(a) in the case of payment of the purchase price to the producer under Articles 47(2), 55 and 65(7), the aid shall be reduced by 1 % per day of delay for one month. After one month, no aid shall be paid; (b) in the case of: -
(i) presentation of proof that the minimum purchase price has been paid under Articles 60(1) and 65(8), (ii) submission of the aid application and the proof of payment under Articles 60(1) and the second subparagraph of Article 64(2) and Article 65(8), (iii) delivery of the alcohol under Article 62(1), (iv) submission of a statement of the quantities of products distilled and products obtained under Article 61(2), (v) submission of a statement of the quantities delivered for fortification under Article 71(3),
the aid shall be reduced by 0.5 % per day of delay for two months. -
-
EUR 0.3626 in Zone A, EUR 0.3019 in Zone B, EUR 0.1811 in Zone C.
-
(a) wine delivered by producers located in regions where alcoholic strength may be increased only by the addition of must who forego all aid made available under Article 34 of Regulation (EEC) No 1493/1999 for the wine year concerned. These producers shall present to the distiller a copy of a statement waiving entitlement to the aid concerned, stamped by the competent authority designated by the Member State; (b) wine taken into a distillery after the dates laid down for the various wine-growing zones in Annex V(G)(7) to Regulation (EC) No 1493/1999 and delivered by producers who provide the competent authorities with satisfactory evidence that during the wine year they have neither increased the alcoholic strength of their table wine by adding sucrose nor lodged an application for aid under Article 34 of that Regulation for their production; (c) wine and categories of wine for which the Member States do not authorise or have not authorised an increase in alcoholic strength for the wine year concerned.
-
(a) the aid to be paid to the distiller, (b) the price to be paid to the distiller for delivery to the intervention agency under Article 30 of Regulation (EC) No 1493/1999 and (c) the EAGGF contribution to expenditure incurred by the intervention agency in taking over alcohol under Article 30 of Regulation (EC) No 1493/1999
-
(a) the heating of glasshouses, (b) the drying of feedingstuffs, (c) the fuelling of heating systems, including those at cement works,
-
(a) the special rules applicable to the tendering procedure and the names and addresses of the intervention agencies concerned, (b) the quantity of alcohol, expressed in hectolitres of alcohol at 100 % vol., covered by the tendering procedure, (c) one or more vats constituting a lot in a given Member State, (d) the minimum price which may be offered, differentiated where appropriate according to the end uses, (e) the amount of the tendering security required under Article 82(5) and the performance guarantee required under Article 84(3)(b).
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(a) the quantity of alcohol to which they relate, broken down by vat and expressed in hectolitres of alcohol at 100 % vol., (b) the number(s) of the vat(s) in which the alcohol concerned is stored, the vats all being situated in the same Member State, (c) the precise industrial use of the alcohol, (d) the type of goods to be exported if the alcohol is intended for export to third countries in the form of manufactured goods.
-
(a) either in proportion to the quantities specified in the tenders concerned, (b) or by dividing that quantity among the tenderers by agreement with them, (c) or by drawing lots.
-
(a) notify the decisions taken under this Article only to those Member States and intervention agencies holding alcohol for which tenders have been accepted, (b) publish the results of the tendering procedure in a simplified form in the Official Journal of the European Communities .
-
(a) obtain the statement of award referred to in paragraph 2 from the intervention agency, (b) provide the intervention agency concerned with proof that a performance security has been lodged to ensure that the alcohol in question is in fact used for the purposes specified in the tender.
-
(a) the formalities for the submission of tenders, (b) the final use and/or destination for which the alcohol is intended, (c) the minimum price which may be offered, (d) the Commission department to which tenders should be sent, (e) the time limit for removal of the alcohol stipulated in Article 91(10) of this Regulation, (f) the formalities for obtaining samples, (g) the payment terms, (h) whether the alcohol is to be denatured.
-
(a) shall immediately issue tenderers with a statement certifying that the tendering security has been lodged for the quantities for which each intervention agency is responsible, (b) shall forward a list of the tendering securities checked and accepted to the Commission not more than two working days after the closing date for submission of tenders.
-
(a) inform tenderers in writing against a receipt if their tenders have not been accepted, (b) notify the Member States holding the alcohol and the successful tenderer of its decision to award the alcohol, (c) publish the results of the tendering procedure in a simplified form in the Official Journal of the European Communities .
-
(a) the intervention agency shall inform the Commission, the storer and the successful tenderer thereof on the same day; (b) the successful tenderer may: -
(i) either agree to take over the lot with the characteristics determined by the analysis, provided the Commission so agrees, (ii) or refuse to take over the lot concerned.
-
-
(a) 15 % in all cases; (b) 0,33 % of the amount remaining after 15 % has been deducted for each day by which the time limit for export has been exceeded.
-
(a) a declaration by the firm stating that it is capable of using at least 50000 hl of alcohol a year; (b) the location of the firm’s administrative offices; (c) the place of establishment and a copy of the plans of the plant where the alcohol is processed into absolute alcohol, and an indication of the annual processing capacity; (d) a copy of the permit, granted by the national authorities of the Member State concerned, to operate the plant; and (e) an assurance by the undertaking that all final purchasers of the alcohol will only use it for the production of fuel in the Community in the form of bio-ethanol.
-
(a) the special rules applicable to the tendering procedure and the names and addresses of the intervention agencies concerned; (b) the quantity of alcohol, expressed in hectolitres of alcohol at 100 % vol, covered by the tendering procedure; (c) the lots; (d) the payment terms; (e) the formalities for obtaining samples; (f) the amount of the tendering security referred to in Article 94(4) and of the performance guarantee referred to in Article 94c(3).
-
(a) the prices offered; (b) the lots requested. (c) the final destination of the alcohol.
-
(a) the quantity of alcohol, expressed in hectolitres of alcohol at 100 % vol., that may be offered for sale, (b) the type of alcohol concerned, (c) the quality of the lots of alcohol, laying down maximum and minimum values for the characteristics referred to in Article 96(4)(d)(i) and (ii) of this Regulation.
-
(a) the location of the lot, including a reference identifying each vat containing the alcohol, and the quantity of alcohol in each vat; (b) the total quantity, expressed in hectolitres of alcohol at 100 % vol. The quantity may vary up to 1 %; (c) the minimum alcoholic strength of the alcohol in each vat, expressed in % vol.; (d) if possible, the quality of the lot, specifying upper and lower limits for the following: -
(i) the acidity, expressed in grams of acetic acid per hectolitre of alcohol at 100 % vol., (ii) the methanol content, expressed in grams per hectolitre of alcohol at 100 % vol.;
-
(e) reference to the intervention measure which gave rise to the production of the alcohol, specifying the relevant Article of Regulation (EC) No 1493/1999.
-
(a) the reference number of the notice of invitation to tender, (b) the name and address of the tenderer, (c) the price proposed, expressed in euros per hectolitre of alcohol at 100 % vol., (d) an undertaking from tenderers to comply with all the rules applicable to the tendering procedure concerned, (e) a statement by tenderers to the effect that: -
(i) they waive all claims in respect of the quality and characteristics of the alcohol awarded to them, (ii) they agree to submit to any checks made on the destination and use of the alcohol, (iii) they accept that it is their responsibility to provide evidence that the alcohol is used as specified in the notice of invitation to tender.
-
-
(a) the tenderer is established in the Community, (b) they relate to the entire lot.
-
1) (a) for the purposes of the tendering security, the primary requirements within the meaning of Article 20 of Regulation (EEC) No 2220/85 shall be that tenders not be withdrawn after the closing date for their submission and that a performance guarantee be lodged; (b) for the purposes of the performance guarantee, the primary requirements within the meaning of Article 20 of Regulation (EEC) No 2220/85 shall be that the alcohol removed be actually used for the purposes specified under the relevant tendering procedure and that the entire quantity of alcohol be physically removed from the stores of each intervention agency concerned within the time allowed.
2) -
(a) The alcohol awarded must be used entirely for the purposes specified in the invitation to tender concerned, allowing for any losses of alcohol during the transport or processing operations required for the final use of the alcohol. Each individual loss of alcohol shall be accepted only if it has been checked at the final destination and, in the case of alcohol for export, at the place where it left the customs territory of the Community, and certified by the competent inspection authority and/or international surveillance firm where such a firm has been appointed under Article 102, provided that such losses are within the limits specified in point (b) below. (b) Where alcohol losses during the operations referred to below exceed the following limits, EUR 96 per hectolitre shall be withheld from the performance guarantee, except in cases of force majeure :-
(i) 0.05 % of the quantities of alcohol stored per month in the case of an alcohol loss due to evaporation, (ii) 0.4 % of the quantities of alcohol removed from storage in the case of an alcohol loss due to one or more land transport operations, (iii) 1 % of the quantities of alcohol removed from storage in the case of alcohol losses due to one or more land transport operations combined with one or more sea or inland waterway transport operations, (iv) 2 % of the quantities of alcohol removed from storage in the case of alcohol losses due to land and sea transport required in connection with a tendering procedure for export of alcohol to one of the third countries listed in Article 86 of this Regulation, (v) 0.9 % of the quantities of alcohol rectified in the case of an alcohol loss due to rectification in the Community, (vi) 0.9 % of the quantities of alcohol dehydrated in the case of an alcohol loss due to dehydration in the Community, (vii) 1.2 % of the quantities of alcohol rectified in the case of an alcohol loss due to rectification in one of the third countries listed in Article 86 to this Regulation, (viii) 1.2 % of the quantities of alcohol dehydrated in the case of an alcohol loss due to dehydration in one of the third countries listed in Article 86 to this Regulation.
The fifth and/or sixth percentage may be added to the second and third percentages. The seventh and/or eighth percentage may be added to the fourth percentage. When applying the abovementioned percentages, the quantities of alcohol shall be determined on the basis of tonnage certificates or similar documents issued by the competent inspection authorities. -
(c) In the case of alcohol awarded for a new industrial use and alcohol awarded under tendering procedures for use as bio-ethanol in the fuel sector in the Community which must be rectified prior to the final use intended, the alcohol removed shall be deemed to have been used entirely for the purpose specified where at least 90 % of the total quantities of alcohol removed under an invitation to tender is used for that purpose. The tenderer who has agreed to purchase the alcohol shall inform the intervention agency of the quantity, destination and use of the products derived from the rectification. However, losses may not exceed the limits specified in point (b).
-
3) -
(a) The tendering security shall be released immediately if the tender has not been accepted or if the successful tenderer has met the requirements laid down in paragraph 1(a). (b) The performance guarantee shall be released immediately by each of the intervention agencies holding alcohol once the successful tenderer provides them each with the proof required in points 2 and 3 and in Title V of Regulation (EEC) No 2220/85, for the relevant quantity removed. (c) Notwithstanding Article 27 of Regulation (EEC) No 2220/85, 10 % of the performance guarantee shall be withheld until the successful tenderer provides each intervention agency concerned with proof that the relevant quantity of alcohol removed has been used, indicating any losses of alcohol in connection with the tendering procedure concerned. If such proof is not produced within 12 months after the date specified for the final use of the alcohol, EUR 96 per hectolitre shall be withheld on the quantities of alcohol lost over and above the limits specified in paragraph 2.
-
-
(a) physical checks on the quantity of alcohol transported, (b) verification of the use made of the alcohol, by frequent spot checks at least once per month, (c) verification of accounts, records, utilisation procedures and stocks.
-
(a) no later than 31 December of the wine year following that in which the contracts were concluded, the quantities of grape must processed into concentrated grape must or rectified concentrated grape must during the period of validity of the contract, and the quantities so obtained; (b) by 5 March of the current wine year at the latest, the quantities of products under contract at 16 February.
-
(a) the quantities of wine, wine lees and fortified wine which have been distilled in the previous month, (b) the quantities of alcohol, broken down into neutral alcohol, raw alcohol and spirits: -
produced during the previous month, taken over by the intervention agencies during the previous month, disposed of by the intervention agencies during the previous month and the percentage of those quantities exported and the selling prices charged, held by the intervention agencies at the end of the previous month.
-
-
(a) the quantities of alcohol physically removed during the previous month under a tendering procedure; (b) the quantities of alcohol physically removed during the previous month following a public sale.
-
(a) the quantities of wine distilled during the previous month; (b) the quantities of alcohol which qualified for secondary aid during the previous month.
-
(a) the number of producers who have received aid; (b) the quantities of wine enriched; (c) the quantities of concentrated grape must and rectified concentrated grape must used for enrichment, expressed in terms of potential alcoholic strength by volume per hectolitre and broken down by the wine-growing zone of origin.
-
(a) the quantities of raw materials covered by aid applications, broken down by type; (b) the quantities of raw materials on which aid has been granted, broken down by type.
-
(a) the quantities of grape must and concentrated grape must covered by aid applications, broken down by wine-growing zone of origin; (b) the quantities of grape must and concentrated grape must on which aid has been granted, broken down by wine-growing zone of origin; (c) the prices paid by manufacturers and operators for the grape must and concentrated grape must.
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(a) no later than 30 April for the previous wine year, the cases where distillers and makers of fortified wine for distillation have failed to fulfil their obligations and the action taken in consequence; (b) 10 days before the end of each quarter, the action taken in response to appeals on the grounds of force majeure and the steps taken in those instances by the competent authorities in cases covered by this Regulation.
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Regulation (EEC) No 1059/83, Regulation (EEC) No 2640/88, Regulation (EEC) No 2641/88, Regulation (EEC) No 2721/88, Regulation (EEC) No 2728/88, Regulation (EEC) No 3105/88.
Concentrated must | Rectified concentrated must | |
---|---|---|
42.93 | ||
43.04 | ||
43.13 | ||
43.23 | ||
43.32 | ||
43.42 | ||
43.52 | ||
43.62 | ||
43.72 | ||
43.81 | ||
43.92 | ||
44.02 | ||
44.12 | ||
44.22 | ||
44.31 | ||
44.41 | ||
44.51 | ||
44.61 | ||
44.71 | ||
44.81 | ||
44.91 | ||
45.01 | ||
45.11 | ||
45.21 | ||
45.30 | ||
45.40 | ||
45.50 | ||
45.61 | ||
45.71 | ||
45.80 | ||
45.91 | ||
46.11 | ||
46.22 | ||
46.32 | ||
46.53 | ||
46.64 | ||
46.74 | ||
46.83 | ||
46.93 | ||
47.03 | ||
47.12 | ||
47.23 | ||
47.34 | ||
47.44 | ||
47.55 | ||
47.65 | ||
47.75 | ||
47.85 | ||
60.56 | ||
60.68 | ||
60.79 | ||
60.91 | ||
61.02 | ||
61.14 | ||
61.25 | ||
61.37 | ||
61.48 | ||
61.60 | ||
61.72 | ||
61.83 | ||
61.94 | ||
62.06 | ||
62.18 | ||
62.28 | ||
62.41 | ||
62.52 | ||
62.64 | ||
62.76 | ||
62.87 | ||
63.10 | ||
63.33 | ||
63.46 | ||
63.58 | ||
63.69 | ||
63.81 | ||
63.93 | ||
64.05 | ||
64.16 | ||
64.28 | ||
64.41 | ||
64.54 | ||
64.66 | ||
64.78 | ||
64.89 | ||
-
(a) Minimum actual alcoholic strength: 10.5 % vol. (b) Maximum volatile acidity: 9 milliequivalents per litre (c) Maximum sulphur dioxide content: 155 milligrams per litre
-
(a) Minimum actual alcoholic strength: 10.5 % vol. (b) Maximum volatile acidity: 11 milliequivalents per litre (c) Maximum sulphur dioxide content: 115 milligrams per litre
No extraneous flavour detectable in the raw material | |
96 % vol. | |
|
1.5 |
|
1.3 |
|
0.5 |
|
0.5 |
|
50 |
|
1.5 |
|
0.1 |
|
Not detectable |
-
(a) the repeatability limit is the value below which the absolute difference between two single test results obtained under the same conditions (same operator, same apparatus, same laboratory and a short interval of time) may be expected to lie with a specified probability; (b) the reproducibility limit is the value below which the absolute difference between two single test results obtained under different conditions (different operators, different apparatus and/or different laboratories and/or different time) may be expected to lie with a specified probability.
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Weigh accurately 59,50 g CoCl 2 .6H2 O, prepare a mixture of 25 ml hydrochloric acid (P 20 = 1,19 g/ml) and 975 ml water,add the cobalt chloride to some of the HCI/water mixture in a 1000 ml volumetric flask and make up to the mark with the rest of the mixture at 20o C.
-
Weigh accurately 45,00 g FeCl 3 .6H2 O, prepare a mixture of 25 ml hydrochloric acid (P 20 = 1,19 g/ml) and 975 ml water and then proceed with the weighed quantity of ferric chloride as for colour solution A.
-
Pipette 10 ml of the sample into a test tube or 50 ml in a Nessler tube, place in water bath at 20 o C,add 1 ml or 5 ml, depending on the sample quantity used, of 1 mmol/l KMnO 4 , solution, mix and leave in the water bath at 20o C,note the time, pipette 10 ml of the colour standard into a test tube of the same diameter or 50 ml of the colour standard into a Nessler tube, observe the change of colour of the sample and compare it with the colour standard against a white background from time to time, note the time at which the colour of the sample becomes the same as that of the colour standard.
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Dissolve 5,0 g powdered p-rosaniline hydrochloride with about 1000 ml hot water in a2000 ml volumetric flask, leave in the water bath until completely dissolved if necessary, dissolve 30 g anhydrous sodium sulphite (or an equivalent quantity of sodium metabisulphite) in circa 200 ml water and add to the cool prosaniline solution, leave to stand for about 10 minutes, add 60 ml hydrochloric acid (p 20 = 1,19 g/ml),where the solution is colourless — a slight degree of brown colouration can be ignored — make up to the mark with water, if necessary filter with a little active carbon over a folded filter to render the solution colourless.
-
(1) The Schiff's reagent should be prepared at least 14 days before it is used. (2) The free SO 2 content in the reagent should be between 2,8 and 6,0 mmol/100 ml, the pH must be 1.Determination of free SO 2 -
Pipette 10 ml Schiff's reagent into a 250 ml Erlenmeyer flask, add 200 ml water, add 5 ml starch solution, titrate with 0,05 mol/l iodine solution to starch end-point,
if the free SO 2 content is outside the indicated range it should either be:-
raised with a calculated quantity of sodium metabisulphite (0,126 g Na 2 SO3 /100 ml reagent per mmol SO2 lacking), or lowered by bubbling air through the reagent.
Calculation of free SO 2 in the reagent.mmol free SO 2 /100 ml reagent:Important: It other methods are used to prepare the Schiff's reagent, the sensitivity of the reagent should be checked so that during the test: -
there is no colouration with the aldehyde-free reference alcohol, the pink colouration should be visible from 0,1 g acetaldehyde per hl alcohol at 100 % vol.
-
(3) Purification of commercial 1-amino-ethanol -
Dissolve 5 g 1-amino-ethanol completely in circa 15 ml absolute ethanol, add circa 50 ml dry diethyl ether (1-amino-ethanol precipitates), leave for several hours in a refrigerator, filter off the crystals and wash with dry diethyl ether, dry for three to four hours in a desiccator over sulphuric acid in a partial vacuum.
Note: The cleaned 1-araino-ethanol must be white; if not, repeat the recrystallisation process. -
-
Weigh 1,3860 g purified and dried 1-amino-ethanol accurately on an analytical balance. Place in a 1000 ml volumetric flask and add aldehyde-free ethanol-free ethanol, make up to the mark at 20o C. The solution content 1 g/l acetaldehyde.Prepare the dilution series in two stages to produce 10 reference solutions containing 0,1 to 1,0 mg acetaldehyde per 100 ml solution. Determine the absorbance values for these reference solutions according to 6.3 and construct graph.
-
Pipette 5 ml of the sample into a colorimetric tube. Add 5 ml water, mix and keep at a constant temperature of 20 o C.At the same time make a blank using 5 ml aldehyde-free ethanol at 96 % vol, add 5 ml water and keep at a temperature of 20 o C.Then add 5 ml Schiff's reagent to each tube, close with ground-glass stoppers and shake well. Keep in water bath for 20 minutes at 20 o C.Put contents into cuvettes. Determine absorbence values at 546 nm.
-
(1) To determine the aldehyde figures it is necessary to check the validity of the calibration curves by comparison with test solution; if not, the calibration curve must be prepared again. (2) Ensure that the blank is always colourless.
-
Weigh 0,2 g indigo carmine, dissolve in 40 ml water and make up to 100 g with ethanol.
-
Weigh 0,2 g phenol red, dissolve in 6 ml sodium hydroxide 0,1 mol/1 and make up to mark with water in a 100 ml volumetric flask.
-
Pipette 100 ml of the sample into the 250 ml round-bottom flask, add boiling stones and briefly heat to boiling in the reflux condenser, add one drop of each of indicator solutions A and B to the hot solution, then titrate with sodium hydroxide 0,01 mol/l until the first signs of change from greenish-yellow to violet.
-
Weigh accurately 1,0 g ethyl acetate on an analytical balance, add ester-free alcohol in a 1000 ml volumetric flask and make up to the mark at 20o C,prepare dilution series in two stages to produce 20 reference solutions containing 0,1 to 2,0 mg ethyl acetate per 100 ml solution, determine absorbence values for the reference solution in accordance with 6.2 and construct a graph.
-
Pipette 10 ml of the sample into test-tubes fitted with ground-glass stoppers, add 2 ml hydroxylamine hydrochloride solution, at the same time prepare a blank using 10 ml ester-free ethanol at 96 % vol and 2 ml hydroxylamine hydrochloride solution, then add 2 ml sodium hydroxide to each solution, close the tubes with ground-glass stoppers and shake well, keep for 15 minutes at 20 o C in a water bath,add 2 ml hydrochloric acid to each tube, shake briefly, add 2 ml ferric chloride solution, mix well, pour contents into cuvettes, Determine absorbence values at 525 nm.
-
Rinse clean cuvettes with sample solution and then pour in the sample; dry the outside of the cuvettes, treat reference cuvette in the same way with n-Hexane and fill, determine absorbence values and construct graph.
Name of successful tenderer: Date of award: Date of refusal or acceptance of the lot by the successful tenderer: